Soluble only in concentrated sulfuric acid.
1348
Typical of an oxygen or nitrogen containing compound.
Peak near 4.2ppm is exchangeable.
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#
Assignments may be 5 Ar (Ph ?), 2 methylenes joined together, 1 OH, NH or SH.
#
dummy ms
#
#
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No extra elements were detected.
212531353941424349264048
Absent are nitrogen, halogen and sulfur containing compounds.
Burnt with a sooty flame leaving no residue.
#
This indicates that the compound is at least partly aromatic.
Below room temperature.
#
True for a liquid.
liquid film
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141922242729423153
The compound is an alcohol and has a monosubstituted benzene ring.
218-221 degrees.
#
#
Optically inactive.
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No chiral centres are present in the unknown.
1.0233
#
A typical value for an organic liquid.
1.524
#
A typical value.
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dummy cmr
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No precipitate formed.
2227282950
Unknown 31 is not an aldehyde or ketone.
A reaction occurred giving a gas (hydrogen).
#
The unknown is an alcohol or a related compound.
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#
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No change was observed.
14
Unknown 31 is not an ester.
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A rapid reaction took place which gave a liquid product.
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The unknown is an alcohol (or an amine).
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#
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Very slow discolourisation occurred on standing.
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The unknown can be slowly oxidised eg an alcohol; it is not unsaturated.
A reaction took place giving an aldehyde.
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Unknown 31 is a primary alcohol.
No colour change was observed.
232850
The compound is not a sugar.
#
#
#
No reaction was observed.
#
The unknown is not unsaturated.
No positive result.
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The compound is not an ether.
No change was noted.
#
Unknown 31 is not a phenol.
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No positive result.
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The compound is not a 1,2-diol.
No positive result.
#
Unknown 31 is not a 1,2-diol.
A rapid reaction took place.
#
The unknown is a primary or secondary alcohol.
## Danger ## violent reaction.
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The compound contains either nitrogen or oxygen.
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#
#
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#
#
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Two phases were seen but no reaction occurred.
#
The unknown is not a low molecular weight secondary or tertiary aliphatic alcoho
No observable change.
#
The unknown is not unsaturated.
No reaction took place.
#
Functional groups like esters, acetals, amides and nitriles are not present.
A rapid reaction occurred.
#
The unknown is an alcohol ( or an amine).
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colourless liquid
010509
203054
6974757684
Colourless solid, m.p. 60-64 degrees.
Solid m.p. 116-119 degrees.
Crystals m.p. 121-124 degrees.
Solid m.p. 105-108 degrees.
Solid with melting range of 78 to 80 degrees.
4
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liquid alcohol
3
1-phenyl-1-propanol
2-phenylethanol
terpineol