The unknown was soluble only in concentrated sulfuric acid.
1348
Typical behavior of neutral, oxygen containing compounds.
Peak at 2ppm is exchangeable. Deuterochloroform is the solvent.
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5 ArH (Ph ?), 1 exchangeable (OH, NH or SH), 6 saturated aliphatic protons.
The molecular ion occurs at 136.
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26
The base peak at 107 is formed by loss of Et (29) from 136.
Lambda max. nm (log absorbance):248 (2.2), 251 (2.3).
#
The compound is conjugated (aromatic).
No extra elements were detected.
212531353941424349264048
The compound does not contain nitrogen, sulfur or halogens.
The unknown burnt with a smoky flame.
#
This indicates unsaturation.
Below room temperature.
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As usual for a liquid.
Thin film.
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141922242729423153
The compound has aromatic character (Ph ?) and OH vibrations.
218-219 degrees.
#
Typical for liquid.
Optically inactive.
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The compound is achiral.
1.006
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A typical value.
1.526
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A typical value.
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Solvent is deuterochloroform.
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14192224272942
4 Ar C's (& 3 H's), methine, methylene, methyl. Symmetry, heteroatom implied.
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No precipitate formed.
2227282950
The compound is not an aldehyde or a ketone.
A rapid reaction which evolved a gas took place.
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The compound contains active hydrogen eg a phenol or alcohol.
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No reaction was noticed.
14
The compound is not an ester.
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A reaction took place which gave an oil.
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The compound could be an alcohol or phenol.
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No reaction was seen within a few minutes.
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The compound contains no readily oxidisable groups.
A reaction occurred giving a ketone.
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A secondary alcohol is present.
No colour change was observed.
232850
The compound is not a sugar.
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No reaction was seen.
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The unknown is not a phenol, alkene or alkyne.
No positive result.
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The compound is not an ether.
No reaction.
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The unknown compound is not a phenol or enol.
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No reaction could be seen.
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This compound is not a polyhydric alcohol.
No positive result.
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The compound is not a 1,2-diol.
Oxidation to a ketone was seen.
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The unknown is a secondary alcohol.
** Danger ** A rapid reaction occurred.
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Typical reaction of oxygen containing compounds.
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A reaction probably occurred but it was difficult to be sure.
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A better test for an alcohol is indicated.
No reaction.
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The unknown is not unsaturated nor is it a phenol.
No reaction could be seen.
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Thecompound is not an acetal, amide, anhydride, nitrile etc.
A reaction occurred to give an oil.
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The unknown is probably an alcohol or phenol.
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colourless liquid
01050920
0
6974
Colourless solid m.p. 56 to 60 degrees
Solid with m.p. range of 100-102 degrees
4
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liquid aromatic alcohol
3
3-methylbenzyl alcohol
1-phenylethanol
1-phenyl-1-propanol