The unknown dissolved only in concentrated sulfuric acid. 1348 This indicates that the unknown is a neutral, oxygen-containing compound. Signal near 2.1 ppm is exchangeable. Deuterochloroform solvent. Ǿ̿» ϛB *fhTi蔶"!ȶ# & # The unknown is a saturated aliphatic alcohol with 12 ( or multiple ) H's. # dummy ms # # # # # No extra elements were detected. 212531353941424349264048 Elements like sulfur, nitrogen and the halogens are absent. The compound burnt with a clear flame and left no residue. # The compound is saturated and not a metal salt. Below room temperature. # A requirement for a liquid. Liquid film ((((((((((('(((''''&&%%%&&'(),-.26=AKR]it{xusssǹ{snljhgjfb[VTPONLIHGFEC@=;9764310///-,+*)))(''&%%%$$$###""""""!!!"!!"#$&&$$$#!! !!""#"""!!! !!!!!!!!!!!!!!"#$&''()++*)(''( (((((())))))***,,,,,.//00124458:>@CGWi~{xvrnie^[XUUY[[[[[Y[^adggd]OICABIQe_QLRXbo|vg_WMpq~ʼzoozm^O@F@:34;54;8,$!!"$',5Ee]G:45:?AABLTYZ[YWTUWZ_`bdfghjkmmmmmmmlljihgfea_]ZVSPKHEC@==>@=82/--,182+%"#&&$" "!%'& 141922242729423153 This compound is a saturated aliphatic alcohol. 129-132 degrees. # A typical value for a liquid. Optically inactive. # The molecule is not chiral. 0.809 # Typical for an organic liquid. 1.409 # A typical value. # # # # # # # dummy cmr # # # # # # # # # # # No precipitate was formed. 2227282950 The compound is not a ketone or an aldehyde. A vigorous reaction with gas evolution took place. # This reaction indicates an active H (eg alcohol, phenol or water if not dry). # # # # # # # # # No change was seen. 14 The unknown is not an ester. # # # # # # # # # # # # # # # A rapid reaction occurred which gave a sweet-smelling liquid. # The unknown is an alcohol which reacted to form an ester (smell). # # # On standing for a long time at room temperature a reaction occurred. # The unknown is saturated but can be slowly oxidised (due to an alcohol ?). An aldehyde was obtained as the product. # Only a primary alcohol can be oxidised to an aldehyde. No colour change was observed. 232850 The unknown is not a sugar. # # # No reaction was observed. # The unknown is not unsaturated nor is it a phenol. No positive result. # The compound is not an ether. No reaction could be seen. # The unknown is not a phenol. # # # # # # # # # # # # # # # No change could be seen. # This liquid is not a 1,2-diol. No positive reaction. # The unknown is not a 1,2-diol. A rapid reaction occurred. # The unknown is a primary or secondary alcohol. A very vigorous reaction took place and a solution was obtained. # This is typical of an oxygen-containing compound. # # # # # # # # # A clear solution was formed. # The unknown is a low molecular weight primary alcohol. No change was noted. # The compound is not a phenol nor is it unsaturated. No reaction took place. # The compound is not an ester, acetal, amide, nitrile etc. A reaction occurred giving a liquid. # The compound is an alcohol (prim. or sec. amines would give solids). # # # # # # # # # # # # # # # # # # colourless liquid 010509 203054 74757684 Solid m.p. 66-69 degrees. Colourless crystals m.p. 164-167 degrees. Solid with melting range of 61 to 63 degrees. Solid m.p. range 55-57 degrees. 3 yNql õli ¯sj|lf liquid aliphatic alcohol 4 2-methyl-3-pentanol 2-methyl-1-butanol Isoamyl alcohol 3-hexanol