Although water insoluble the unknown dissolved in dilute HCl. 1348 Typical of a compound containing a basic functional group. Peak near 3.2ppm is exchangeable. Solvent is deuterochloroform. ŭ ̹P Y M$" # # Ratio 4 aromatic, 2 replaceable, 3 as methyl. ODD number (N present or double). # dummy ms # # # # # Nitrogen was found. 264048 There are no halides or sulfur in this compound. The compound burned with a smoky flame; no residue remained. # This compound is unsaturated or aromatic. It is not a metallic salt. Below room temperature. # Typical behavior for a liquid. Liquid film ./...,/..--,,*)('())*)(((''()*++,...,-.149=BOeýznfhnsw~zn_HD??>AHN[hy}oq|t}{zT@;7/.///16=@.*,,,./2598/*))('('&%%)**('%%%%%&&%%'()('%$#$&&'''&&&%%%%&''&%%%&*)(()(((((**+-.136:<:98;?CDC:0////.+)*+-///..0268742-,,,.0000369=BHK MU]n~²qhYLGDEIW`nȶà_K>533660+*+.14=FM]`PIWqufD/&&&+?Yb?1+(%$%+8DUS:" "$&*.16=HU_feIBDHMRW^iszu{wqkf_Zryotrh`YSNLJGFDCKlncfcbfi 141922242729423153 A primary amine is present in this aromatic compound. 199-201 degrees. # Typical value for a liquid. Optically inactive. # The unknown is achiral. 1.005 # A typical value. 1.569 # A typical value. # # # # # # # dummy cmr # # # # # # # # # # # No precipitate was formed. 2227282950 The unknown is not an aldehyde nor a ketone. No positive result. 3344454651 The unknown is not an alcohol, phenol or other active H containing compound. A bright coloured azo dye was formed. # This compound is a primary aromatic amine. # # # # # # No reaction. 14 The compound is not an ester. No reaction was observed. # Nitro groups are absent from this compound. # # # # # # # # # # # # A vigorous reaction took place to give a solid. # The compound is a primary or secondary amine. No positive result. # The unknown is not an amide or nitrile. No reaction was seen. # The compound is not unsaturated nor easily oxidised. # # # No colour change was observed. 232850 This unknown is not a sugar. No change was noted. # The unknown does not contain a nitro group. No reaction took place. # The unknown is not a phenol nor is it unsaturated. No positive result. # The compound is not an ether. No change was observed. # This compound is not a phenol. No reaction was observed. # This compound is a primary amine. # # # A reaction occurred; the product was base soluble. # The unknown is a primary amine. No change was noticed. # The compound is not an amino acid. A sickening smell was noticed. You left and went home. # The compound is a primary amine. # # # # # # # # # ****** Danger ****** A very vigorous reaction. # Typical behavior for an amine. # # # No positive result. # This unknown is not a secondary amine. # # # # # # No reaction was seen. # The unknown is not unsaturated nor is it a phenol. No reaction took place. # The compound is not a nitrile, amide, ester, acetal etc. A rapid reaction occurred which gave a solid. # The unknown could be an amine, amino acid, phenol or maybe an alcohol. # # # # # # # # # # # # # # # # # # colourless liquid 010509 214143 677078899092 Solid m.p. 110-112 degrees. Colourless solid m.p.range 136-137 degrees. Solid m.p. 144-146 degrees. Colourless crystals m.p. 124-126 degrees. Solid m.p. 183-186 degrees. Yellow crystals m.p. 211-215 degrees. 4 ik yk yk ybġf primary aromatic amine 2 o-toluidine m-toluidine