The compound dissolved in both water (giving a basic solution) and ether.
1348
Typical of low molecular weight amines.
Peak near 1.1ppm is exchangeable. Solvent is deuterochloroform.
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#
Ratio suggests 3 alkene to 2 other deshielded protons and 2 exchangeable ones.
Molecular ion is at 57.
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26
Odd molecular ion means an odd number of N must be present.
The compound was UV transparent.
#
The unknown is not conjugated.
Nitrogen was found.
264048
No sulfur or halogens are present.
The liquid burnt with a somewhat smoky flame leaving no residue.
#
This suggests unsaturation and non-salt like character.
Below room temperature.
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As expected for a liquid.
Thin film.
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141922242729423153
Peaks due to an amine and an alkene can be seen.
55 to 58 degrees.
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A low boiling point liquid suggesting a low molecular weight.
Optically inactive.
#
The compound is achiral.
0.760
#
Fairly low for an organic liquid.
1.420
#
Typical value.
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Solvent is deuterochloroform.
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14192224272942
3 C's (& 7 H's). Monosubstituted alkene. Odd no. H (heteroatom or symmetry ?).
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No precipitate was formed.
2227282950
The compound is not an aldehyde nor a ketone.
A vigorous reaction took place.
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The unknown contains a reactive OH or NH.
A vigorous reaction with gas evolution occurred even at low temperature.
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The unknown is a primary aliphatic amine or an unsubstituted amide.
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No colour change was seen.
14
The compound is not an ester.
No change was seen.
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The compound has no nitro groups.
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A vigorous reaction yielding a solid took place.
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The unknown is an alcohol or amine (primary or secondary).
No apparent reaction could be seen.
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The compound is not an amide nor a nitrile.
A reaction was observed.
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The compound could be unsaturated.
No positive result was seen.
#
The unknown is not an alcohol.
No colour change was observed.
232850
The unknown is not a sugar.
No positive result.
#
The compound has no nitro groups.
A reaction occurred; no HBr gas was evolved.
#
The unknown compound is unsaturated.
No positive result was obtained.
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The compound is not an ether.
No reaction was noticed.
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This compound is not a phenol nor an enol.
A violet-red colour formed.
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The unknown is a primary amine.
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A reaction occurred giving a base-soluble solid product.
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The unknown compound is a primary amine.
No colour change was seen.
#
The unknown is not an amino acid.
Nauseating odour - even worse than a rotting fish smell.
#
This behaviour is typical of primary amines.
No useful result was noticed.
#
The unknown is not a 1,2-diol.
No positive result was obtained.
#
This compound is not a 1,2-diol.
No apparent reaction was noticed.
#
The unknown is not a primary or secondary alcohol.
** Danger ** A very rapid reaction took place.
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Typical of N- and/or O-containing compounds.
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No positive result.
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The compound is not a secondary amine.
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No positive result was obtained.
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This compound is not an alcohol.
A reaction took place with discharge of the reagent's colour.
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The compound could be unsaturated or phenolic.
No reaction could be seen.
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The compound is not an acetal, amide, anhydride, ester or nitrile etc.
A rapid reaction occurred and a solid was formed.
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The unknown could be an alcohol, amino acid or amine (primary or secondary).
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fishy-smelling liquid
010509
214143
70899092
Solid m.p. 97-99 degrees
Oily solid m.p. 39-42 degrees
Colourless solid m.p. 63-66 degrees
Yellow crystals m.p. 138-140 degrees
3
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liquid primary amine
3
allylamine
sec-butylamine
isobutylamine